JPH0449219B2 - - Google Patents
Info
- Publication number
- JPH0449219B2 JPH0449219B2 JP62249065A JP24906587A JPH0449219B2 JP H0449219 B2 JPH0449219 B2 JP H0449219B2 JP 62249065 A JP62249065 A JP 62249065A JP 24906587 A JP24906587 A JP 24906587A JP H0449219 B2 JPH0449219 B2 JP H0449219B2
- Authority
- JP
- Japan
- Prior art keywords
- ions
- quadrupole
- mass
- ion
- motion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000002500 ions Chemical class 0.000 claims description 209
- 230000033001 locomotion Effects 0.000 claims description 79
- 230000005284 excitation Effects 0.000 claims description 45
- 238000000034 method Methods 0.000 claims description 40
- 230000005684 electric field Effects 0.000 claims description 34
- 238000004949 mass spectrometry Methods 0.000 claims description 18
- 238000009826 distribution Methods 0.000 claims description 3
- 230000004044 response Effects 0.000 claims description 3
- 230000005686 electrostatic field Effects 0.000 claims description 2
- 230000001939 inductive effect Effects 0.000 claims 1
- 238000001514 detection method Methods 0.000 description 24
- 238000004458 analytical method Methods 0.000 description 21
- 238000005040 ion trap Methods 0.000 description 18
- 239000003990 capacitor Substances 0.000 description 14
- 230000001052 transient effect Effects 0.000 description 13
- 239000000243 solution Substances 0.000 description 12
- 230000001427 coherent effect Effects 0.000 description 11
- 230000008878 coupling Effects 0.000 description 10
- 238000010168 coupling process Methods 0.000 description 10
- 238000005859 coupling reaction Methods 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 9
- 238000001228 spectrum Methods 0.000 description 9
- 238000003384 imaging method Methods 0.000 description 7
- 238000001819 mass spectrum Methods 0.000 description 7
- 238000006073 displacement reaction Methods 0.000 description 6
- 239000000470 constituent Substances 0.000 description 5
- 230000010355 oscillation Effects 0.000 description 5
- 230000003534 oscillatory effect Effects 0.000 description 5
- 238000005173 quadrupole mass spectroscopy Methods 0.000 description 4
- 238000013459 approach Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 238000005070 sampling Methods 0.000 description 3
- 230000003595 spectral effect Effects 0.000 description 3
- 238000012935 Averaging Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000010894 electron beam technology Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 238000004611 spectroscopical analysis Methods 0.000 description 2
- 238000010183 spectrum analysis Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 238000004885 tandem mass spectrometry Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 230000002238 attenuated effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 238000001269 time-of-flight mass spectrometry Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/26—Mass spectrometers or separator tubes
- H01J49/34—Dynamic spectrometers
- H01J49/42—Stability-of-path spectrometers, e.g. monopole, quadrupole, multipole, farvitrons
- H01J49/426—Methods for controlling ions
- H01J49/427—Ejection and selection methods
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/025—Detectors specially adapted to particle spectrometers
- H01J49/027—Detectors specially adapted to particle spectrometers detecting image current induced by the movement of charged particles
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Electron Tubes For Measurement (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US914016 | 1986-10-01 | ||
| US06/914,016 US4755670A (en) | 1986-10-01 | 1986-10-01 | Fourtier transform quadrupole mass spectrometer and method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS63276863A JPS63276863A (ja) | 1988-11-15 |
| JPH0449219B2 true JPH0449219B2 (en]) | 1992-08-10 |
Family
ID=25433811
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62249065A Granted JPS63276863A (ja) | 1986-10-01 | 1987-10-01 | フーリエ変換四極子質量分析計及び質量分析法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4755670A (en]) |
| EP (1) | EP0262928B1 (en]) |
| JP (1) | JPS63276863A (en]) |
| CA (1) | CA1266924A (en]) |
| DE (1) | DE3784428T2 (en]) |
Families Citing this family (92)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02103856A (ja) * | 1988-06-03 | 1990-04-16 | Finnigan Corp | イオントラップ型質量分析計の操作方法 |
| US4990775A (en) * | 1988-06-06 | 1991-02-05 | University Of Delaware | Resolution improvement in an ion cyclotron resonance mass spectrometer |
| FR2634063B1 (fr) * | 1988-07-07 | 1991-05-10 | Univ Metz | Interface microsonde laser pour spectrometre de masse |
| JPH061678B2 (ja) * | 1988-11-24 | 1994-01-05 | 工業技術院長 | 外部共振回路型ｒｆｑ加速器 |
| US4956788A (en) * | 1988-11-28 | 1990-09-11 | University Of The Pacific | PC-based FT/ICR system |
| US4990856A (en) * | 1989-01-23 | 1991-02-05 | Varian Associates, Inc. | Mass analysis apparatus and method |
| ATE101942T1 (de) * | 1989-02-18 | 1994-03-15 | Bruker Franzen Analytik Gmbh | Verfahren und geraet zur massenbestimmung von proben mittels eines quistors. |
| US4945234A (en) * | 1989-05-19 | 1990-07-31 | Extrel Ftms, Inc. | Method and apparatus for producing an arbitrary excitation spectrum for Fourier transform mass spectrometry |
| US5013912A (en) * | 1989-07-14 | 1991-05-07 | University Of The Pacific | General phase modulation method for stored waveform inverse fourier transform excitation for fourier transform ion cyclotron resonance mass spectrometry |
| US5015848A (en) * | 1989-10-13 | 1991-05-14 | Southwest Sciences, Incorporated | Mass spectroscopic apparatus and method |
| US5283436A (en) * | 1990-01-08 | 1994-02-01 | Bruker-Franzen Analytik Gmbh | Generation of an exact three-dimensional quadrupole electric field and superposition of a homogeneous electric field in trapping-exciting mass spectrometer (TEMS) |
| US4982088A (en) * | 1990-02-02 | 1991-01-01 | California Institute Of Technology | Method and apparatus for highly sensitive spectroscopy of trapped ions |
| US5233190A (en) * | 1990-03-16 | 1993-08-03 | Leybold Inficon Inc. | Fourier transform molecular spectrometer |
| JP3002521B2 (ja) * | 1990-10-22 | 2000-01-24 | 日本原子力研究所 | 四重極型質量分析計 |
| US5206506A (en) * | 1991-02-12 | 1993-04-27 | Kirchner Nicholas J | Ion processing: control and analysis |
| US5196699A (en) * | 1991-02-28 | 1993-03-23 | Teledyne Mec | Chemical ionization mass spectrometry method using notch filter |
| US5173604A (en) * | 1991-02-28 | 1992-12-22 | Teledyne Cme | Mass spectrometry method with non-consecutive mass order scan |
| US5105081A (en) * | 1991-02-28 | 1992-04-14 | Teledyne Cme | Mass spectrometry method and apparatus employing in-trap ion detection |
| US5134286A (en) * | 1991-02-28 | 1992-07-28 | Teledyne Cme | Mass spectrometry method using notch filter |
| JPH0774838B2 (ja) * | 1991-03-26 | 1995-08-09 | 工業技術院長 | 荷電粒子の捕獲方法及び装置 |
| US5179278A (en) * | 1991-08-23 | 1993-01-12 | Mds Health Group Limited | Multipole inlet system for ion traps |
| US5206509A (en) * | 1991-12-11 | 1993-04-27 | Martin Marietta Energy Systems, Inc. | Universal collisional activation ion trap mass spectrometry |
| DE4142870C2 (de) * | 1991-12-23 | 1995-03-16 | Bruker Franzen Analytik Gmbh | Verfahren für phasenrichtiges Messen der Ionen aus Ionenfallen-Massenspektrometern |
| US5272337A (en) * | 1992-04-08 | 1993-12-21 | Martin Marietta Energy Systems, Inc. | Sample introducing apparatus and sample modules for mass spectrometer |
| JPH07112539B2 (ja) * | 1992-04-15 | 1995-12-06 | 工業技術院長 | 微小粒子の作製方法及びその装置 |
| US5248882A (en) * | 1992-05-28 | 1993-09-28 | Extrel Ftms, Inc. | Method and apparatus for providing tailored excitation as in Fourier transform mass spectrometry |
| US5532140A (en) * | 1994-03-23 | 1996-07-02 | The United States Of America As Represented By The Secretary Of The Army | Method and apparatus for suspending microparticles |
| US5420425A (en) * | 1994-05-27 | 1995-05-30 | Finnigan Corporation | Ion trap mass spectrometer system and method |
| US5783824A (en) * | 1995-04-03 | 1998-07-21 | Hitachi, Ltd. | Ion trapping mass spectrometry apparatus |
| JP3495512B2 (ja) * | 1996-07-02 | 2004-02-09 | 株式会社日立製作所 | イオントラップ質量分析装置 |
| JP3509267B2 (ja) * | 1995-04-03 | 2004-03-22 | 株式会社日立製作所 | イオントラップ質量分析方法および装置 |
| DE69536105D1 (de) * | 1995-07-03 | 2010-10-28 | Hitachi Ltd | Massenspektrometer |
| JP3385327B2 (ja) * | 1995-12-13 | 2003-03-10 | 株式会社日立製作所 | 三次元四重極質量分析装置 |
| US5625186A (en) * | 1996-03-21 | 1997-04-29 | Purdue Research Foundation | Non-destructive ion trap mass spectrometer and method |
| US5734162A (en) * | 1996-04-30 | 1998-03-31 | Hewlett Packard Company | Method and apparatus for selectively trapping ions into a quadrupole trap |
| CA2255188C (en) | 1998-12-02 | 2008-11-18 | University Of British Columbia | Method and apparatus for multiple stages of mass spectrometry |
| JP2003507874A (ja) * | 1999-08-26 | 2003-02-25 | ユニバーシティ オブ ニュー ハンプシャー | 多段型の質量分析計 |
| US6452168B1 (en) | 1999-09-15 | 2002-09-17 | Ut-Battelle, Llc | Apparatus and methods for continuous beam fourier transform mass spectrometry |
| US6153880A (en) * | 1999-09-30 | 2000-11-28 | Agilent Technologies, Inc. | Method and apparatus for performance improvement of mass spectrometers using dynamic ion optics |
| GB9924722D0 (en) * | 1999-10-19 | 1999-12-22 | Shimadzu Res Lab Europe Ltd | Methods and apparatus for driving a quadrupole device |
| US6528784B1 (en) | 1999-12-03 | 2003-03-04 | Thermo Finnigan Llc | Mass spectrometer system including a double ion guide interface and method of operation |
| US6403955B1 (en) | 2000-04-26 | 2002-06-11 | Thermo Finnigan Llc | Linear quadrupole mass spectrometer |
| US6570153B1 (en) * | 2000-10-18 | 2003-05-27 | Agilent Technologies, Inc. | Tandem mass spectrometry using a single quadrupole mass analyzer |
| JP4303108B2 (ja) * | 2001-08-30 | 2009-07-29 | エムディーエス インコーポレイテッド ドゥーイング ビジネス アズ エムディーエス サイエックス | リニアイオントラップ型質量分析計における空間電荷低減方法 |
| WO2003041116A1 (fr) * | 2001-11-07 | 2003-05-15 | Hitachi High-Technologies Corporation | Spectrometrie de masse et spectrometre de masse a piege a ions |
| US6797950B2 (en) | 2002-02-04 | 2004-09-28 | Thermo Finnegan Llc | Two-dimensional quadrupole ion trap operated as a mass spectrometer |
| JP3951741B2 (ja) * | 2002-02-27 | 2007-08-01 | 株式会社日立製作所 | 電荷調整方法とその装置、および質量分析装置 |
| US6703607B2 (en) * | 2002-05-30 | 2004-03-09 | Mds Inc. | Axial ejection resolution in multipole mass spectrometers |
| WO2004035169A2 (en) * | 2002-10-15 | 2004-04-29 | The Regents Of The University Of Michigan | Multidimensional protein separation system |
| US7019290B2 (en) * | 2003-05-30 | 2006-03-28 | Applera Corporation | System and method for modifying the fringing fields of a radio frequency multipole |
| US7026613B2 (en) * | 2004-01-23 | 2006-04-11 | Thermo Finnigan Llc | Confining positive and negative ions with fast oscillating electric potentials |
| US7078684B2 (en) * | 2004-02-05 | 2006-07-18 | Florida State University | High resolution fourier transform ion cyclotron resonance (FT-ICR) mass spectrometry methods and apparatus |
| US7247855B2 (en) * | 2004-03-09 | 2007-07-24 | United States Of America As Represented By The Secretary Of The Army | Portable nuclear detector |
| US7034293B2 (en) * | 2004-05-26 | 2006-04-25 | Varian, Inc. | Linear ion trap apparatus and method utilizing an asymmetrical trapping field |
| GB0416288D0 (en) * | 2004-07-21 | 2004-08-25 | Micromass Ltd | Mass spectrometer |
| GB2472951B (en) * | 2004-11-29 | 2011-04-27 | Thermo Finnigan Llc | Method of processing mass spectrometry data |
| US7183545B2 (en) * | 2005-03-15 | 2007-02-27 | Agilent Technologies, Inc. | Multipole ion mass filter having rotating electric field |
| WO2007080857A1 (ja) * | 2006-01-16 | 2007-07-19 | National University Corporation Kobe University | 気体核磁気共鳴装置 |
| US7381947B2 (en) * | 2006-05-05 | 2008-06-03 | Thermo Finnigan Llc | Electrode networks for parallel ion traps |
| DE102007034232B4 (de) * | 2007-07-23 | 2012-03-01 | Bruker Daltonik Gmbh | Dreidimensionale Hochfrequenz-Ionenfallen hoher Einfangeffizienz |
| US8399827B1 (en) * | 2007-09-10 | 2013-03-19 | Cedars-Sinai Medical Center | Mass spectrometry systems |
| US7989765B2 (en) * | 2007-11-30 | 2011-08-02 | Agilent Technologies, Inc. | Method and apparatus for trapping ions |
| US8334506B2 (en) * | 2007-12-10 | 2012-12-18 | 1St Detect Corporation | End cap voltage control of ion traps |
| DE102008015000B4 (de) * | 2008-03-19 | 2015-04-09 | Bruker Daltonik Gmbh | Verfahren zur Messung von Ionenmobilitätsspektren |
| GB2463633B (en) | 2008-05-15 | 2013-02-27 | Thermo Fisher Scient Bremen | MS/MS data processing |
| US7973277B2 (en) | 2008-05-27 | 2011-07-05 | 1St Detect Corporation | Driving a mass spectrometer ion trap or mass filter |
| EP2285473A1 (en) * | 2008-05-30 | 2011-02-23 | Purdue Research Foundation | Non-destructive, high order harmonic ion motion image current detection |
| EP2294603A4 (en) * | 2008-06-09 | 2017-01-18 | DH Technologies Development Pte. Ltd. | A multipole ion guide for providing an axial electric field whose strength increases with radial position, and a method of operating a multipole ion guide having such an axial electric field |
| WO2009149546A1 (en) | 2008-06-09 | 2009-12-17 | Mds Analytical Technologies | Method of operating tandem ion traps |
| US8822916B2 (en) | 2008-06-09 | 2014-09-02 | Dh Technologies Development Pte. Ltd. | Method of operating tandem ion traps |
| CN105606691B (zh) | 2009-04-30 | 2018-12-28 | 普度研究基金会 | 分析样品中的蛋白质或肽的方法 |
| US9500572B2 (en) | 2009-04-30 | 2016-11-22 | Purdue Research Foundation | Sample dispenser including an internal standard and methods of use thereof |
| US8704167B2 (en) | 2009-04-30 | 2014-04-22 | Purdue Research Foundation | Mass spectrometry analysis of microorganisms in samples |
| EP2489061B1 (en) * | 2009-10-14 | 2019-02-27 | Bruker Daltonik GmbH | Ion cyclotron resonance measuring cells with harmonic trapping potential |
| CA2779747C (en) * | 2009-11-16 | 2017-11-07 | Dh Technologies Development Pte. Ltd. | Apparatus for providing power to a multipole in a mass spectrometer |
| US9589781B2 (en) * | 2010-12-17 | 2017-03-07 | Shimadzu Corporation | Ion guide and mass spectrometer |
| US9157921B2 (en) | 2011-05-18 | 2015-10-13 | Purdue Research Foundation | Method for diagnosing abnormality in tissue samples by combination of mass spectral and optical imaging |
| US9546979B2 (en) | 2011-05-18 | 2017-01-17 | Purdue Research Foundation | Analyzing a metabolite level in a tissue sample using DESI |
| US8895918B2 (en) | 2011-06-03 | 2014-11-25 | Purdue Research Foundation | Ion generation using modified wetted porous materials |
| CN104956462B (zh) | 2013-01-31 | 2017-10-10 | 普度研究基金会 | 用于分析所提取样本的系统和方法 |
| CN108287209B (zh) | 2013-01-31 | 2021-01-26 | 普度研究基金会 | 分析原油的方法 |
| DE102013208959A1 (de) * | 2013-05-15 | 2014-11-20 | Carl Zeiss Microscopy Gmbh | Vorrichtung zur massenselektiven Bestimmung eines Ions |
| WO2014209474A1 (en) | 2013-06-25 | 2014-12-31 | Purdue Research Foundation | Mass spectrometry analysis of microorganisms in samples |
| US9117646B2 (en) * | 2013-10-04 | 2015-08-25 | Thermo Finnigan Llc | Method and apparatus for a combined linear ion trap and quadrupole mass filter |
| DE102014003356A1 (de) | 2014-03-06 | 2015-09-10 | Gregor Quiring | Vorrichtung zur Ionentrennung durch selektive Beschleunigung |
| US9786478B2 (en) | 2014-12-05 | 2017-10-10 | Purdue Research Foundation | Zero voltage mass spectrometry probes and systems |
| CN107960130A (zh) | 2015-02-06 | 2018-04-24 | 普度研究基金会 | 探针、系统、盒及其使用方法 |
| US10446384B2 (en) * | 2015-04-25 | 2019-10-15 | Dh Technologies Development Pte. Ltd. | Fourier transform mass spectrometer |
| JP7103133B2 (ja) * | 2018-10-02 | 2022-07-20 | 日本精工株式会社 | 転がり軸受の異常診断方法及び異常診断装置、センサユニット、並びに転がり軸受の異常診断システム |
| JP7127009B2 (ja) * | 2019-12-04 | 2022-08-29 | 日本電子株式会社 | 質量分析装置 |
| EP4078651A1 (en) * | 2019-12-17 | 2022-10-26 | DH Technologies Development Pte. Ltd. | Fourier transform quadrupole calibration method |
| GB2613601A (en) * | 2021-12-08 | 2023-06-14 | Edwards Vacuum Llc | Ion trap and method for detecting ions in an ion trap |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT528250A (en]) * | 1953-12-24 | |||
| US3537939A (en) * | 1967-05-01 | 1970-11-03 | Nat Gypsum Co | Splicing apparatus for continuously advancing webs |
| US3527939A (en) * | 1968-08-29 | 1970-09-08 | Gen Electric | Three-dimensional quadrupole mass spectrometer and gauge |
| US3937955A (en) * | 1974-10-15 | 1976-02-10 | Nicolet Technology Corporation | Fourier transform ion cyclotron resonance spectroscopy method and apparatus |
| US4540884A (en) * | 1982-12-29 | 1985-09-10 | Finnigan Corporation | Method of mass analyzing a sample by use of a quadrupole ion trap |
| GB8305228D0 (en) * | 1983-02-25 | 1983-03-30 | Vg Instr Ltd | Operating quadrupole mass spectrometers |
| US4650999A (en) * | 1984-10-22 | 1987-03-17 | Finnigan Corporation | Method of mass analyzing a sample over a wide mass range by use of a quadrupole ion trap |
| EP0409362B1 (en) * | 1985-05-24 | 1995-04-19 | Finnigan Corporation | Method of operating an ion trap |
-
1986
- 1986-10-01 US US06/914,016 patent/US4755670A/en not_active Expired - Lifetime
-
1987
- 1987-09-29 EP EP87308624A patent/EP0262928B1/en not_active Expired - Lifetime
- 1987-09-29 DE DE8787308624T patent/DE3784428T2/de not_active Expired - Fee Related
- 1987-09-30 CA CA000548212A patent/CA1266924A/en not_active Expired
- 1987-10-01 JP JP62249065A patent/JPS63276863A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DE3784428D1 (de) | 1993-04-08 |
| DE3784428T2 (de) | 1993-09-23 |
| US4755670A (en) | 1988-07-05 |
| EP0262928A3 (en) | 1989-12-13 |
| EP0262928A2 (en) | 1988-04-06 |
| JPS63276863A (ja) | 1988-11-15 |
| CA1266924A (en) | 1990-03-20 |
| EP0262928B1 (en) | 1993-03-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| LAPS | Cancellation because of no payment of annual fees |